2021 №12 (06) DOI of Article
2021 №12 (08)

The Paton Welding Journal 2021 #12
The Paton Welding Journal, 2021, #12, 41-48 pages

Producing Fe-based nanoparticles in NaCl matrix by the method of EB-PVD on a rotating substrate

Yu.A. Kurapov, V.O. Osokin, G.G. Didikin, L.A. Krushynska, S.E. Lytvyn, V.V. Boretskyi

E.O. Paton Electric Welding Institute of the NAS of Ukraine 11 Kazymyr Malevych Str., 03150, Kyiv, Ukraine. E-mail:

The paper gives the results on the features of formation of a microlayered structure of NaCl–Fe composite and the possibility of producing iron nanoparticles of different size on a rotating substrate by EB-PVD method with peripheral position of evaporation material sources relative to the substrate rotation axis. It is shown that the layer thickness is determined by the substrate rotation speed. It is found that Fe nanoparticles are present in NaCl matrix in the form of Fe3O4 oxide.
Keywords: electron beam evaporation, condensation, EB-PVD, composite, nanoparticles, iron oxide, phase composition

Received 15.09.2021
Accepted: 24.12.2021


1. Salata, O.V. (2004) Applications of nanoparticles in biology and medicine. J. of Nanotechnology, 2, 3-8. http://www.nanobiotechnology. com/content/2/1/3
2. Movchan, B.A., Kurapov, Yu.A., Didikin, G.G. et al. (2011) Regulation of composition and structure of Fe-O system nanoparticles in electron beam evaporation of Fe3O4. Poroshkovaya Metallurgiya, 50(3-4), (478), 56-63 [in Russian].
3. Kurapov, Yu.A., Litvin, S.E., Romanenko, S.M. (2013) Structure and thermal stability of Ti-NaCl condensates deposited from the vapour phase in vacuum. Nanostructured Materials Sci., 1, 55-62. view.jsp?id=2
4. Kurapov, Yu.A., Litvin, S.E., Didikin, G.G., Romanenko, S.M. (2011) Structure of two-phase condensates Cu-NaCl deposited from vapor phase in vacuum. Sovrem. Elektrometall., 2, 19-22 [in Russian]. https://patonpublishinghouse. com/eng/journals/sem/2011/02/05
5. Kurapov, Yu.A., Romanenko, S.M., Didikin, G.G., Oranskaya, E.I. (2017) Controllable synthesis of iron oxide nanoparticles in porous NaCl matrix. Materials Research Express, 4(3), 035031.
6. Paton, B.E., Movchan, B.O., Kurapov, Yu.A., Yakovchuk, K.Yu. (2010) Method of producing of metal-oxygen system nanoparticles with specified composition by electron beam evaporation and condensation in vacuum. Pat. 92556, Ukraine [in Ukrainian]. php?action=viewdetails&IdClaim=151646'); ?>
7. Grechanyuk, M.I., Osokin, V.O., Afanasiev, I.B. et al. (2002) Method of producing of porous materials. Pat. 46855, Ukraine [in Ukrainian].
8. Grechanyuk, N.I., Osokin, V.A., Grechanyuk, I. N. et al. (2006) Composite materials on base of copper and molybdenum condensed from vapor phase, for electric contacts. Pt 2: Fundamentals of electron beam technology for producing materials for electric contacts. Advances in Electrometallurgy, 2, 8-17.
9. Osokin, V.O., Kurapov, Yu.A., Boretsky, V.V. et al. (2021) Producing of Fe, Cu, Ag nanoparticles in NaCl matrix on rotating substrate by EB-PVD method. In: Abstr. of Pap. of Int. Conf. on Modern Technologies of Joining of Materials. Ed. by L.M. Lobanov. Kyiv, IAW [in Russian]. https://patonpublishinghouse. com/proceedings/stzm2021.pdf'); ?>
10. Movchan, B.A. (2006) Inorganic materials and coating produced by EBPVD. Surf. Eng., 22, 35-46.
11. Movchan, B.A., Demchishin, A.V. (1969) Study of structure and properties of thick vacuum condensates of nickel, titanium, tungsten, aluminium oxide and zirconium dioxide. Fizika Metallov i Metallovedenie, 28(4), 653-660 [in Russian].
12. Kurapov, Y.A., Vazhnichaya, E.M., Litvin, S.E. et al. (2019) Physical synthesis of iron oxide nanoparticles and their biological activity in vivo. SN Applied Sci., 1(1), 1-102.
13. Kurapov, Yu.A., Movchan, B.A., Litvin, S.E. et al. (2011) Effect of iron concentration on the adsorptive capacity of iron oxide nanoparticles in the porous NaCl matrix in relation to atmospheric oxygen. Advances in Electrometallurgy, 9(1), 29-32.