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2021 №03 (03) DOI of Article
10.37434/sem2021.03.04
2021 №03 (05)

Electrometallurgy Today 2021 #03
Electrometallurgy Today (Sovremennaya Elektrometallurgiya), 2021, #3, 19-27 pages

Receive Fe-based nanoparticles in a nacl matrix by EB-PVD on a rotating substrate

Yu.A. Kurapov, V.O. Osokin, G.G. Didikin, L.A. Krushynska, S.Ye. Lytvyn, V.V. Boretskyi


E.O. Paton Electric Welding Institute of the NAS of Ukraine. 11 Kazymyr Malevych Str., Kyiv, 03150, Ukraine. E-mail: office@paton.kiev.ua

Abstract
The results of the peculiarities of the formation of the microlayer structure of the NaCl–Fe composite and the possibility of obtaining iron nanoparticles of different sizes on a rotating substrate by EB-PVD with a peripheral relative to the axis of rotation of the substrate location of sources of evaporating materials. It is shown that the thickness of the layers is determined by the speed of rotation of the substrate. It was found that iron nanoparticles in the matrix of sodium chloride are in the form of Fe3O4 oxide. Ref. 13, Tabl. 7, Fig. 8.
Keywords: electron beam evaporation; condensation; EB-PVD; composite; nanoparticles; iron oxide; phase composition

Received

References

1. Salata, O.V. (2004) Applications of nanoparticles in biology and medicine. J. of Nanotechnology, 2, 3-8. https://doi.org/10.1186/1477-3155-2-3
2. Movchan, B.A., Kurapov, Yu.A., Didikin, G.G. et al. (2011) Regulation of composition and structure of Fe-O system nanoparticles in electron beam evaporation of Fe3O4. Poroshkovaya Metallurgiya, 50(3-4), (478), 56-63 [in Russian]. https://doi.org/10.1007/s11106-011-9314-0
3. Kurapov, Yu.A., Litvin, S.E., Romanenko, S.M. (2013) Structure and thermal stability of Ti-NaCl condensates deposited from the vapour phase in vacuum. Nanostructured Materials Sci., 1, 55-62. http://www.materials.kiev.ua/science/edition_ view.jsp?id=2
4. Kurapov, Yu.A., Litvin, S.E., Didikin, G.G., Romanenko, S.M. (2011) Structure of two-phase condensates Cu-NaCl deposited from vapor phase in vacuum. Sovrem. Elektrometall., 2, 19-22 [in Russian]. https://patonpublishinghouse. com/eng/journals/sem/2011/02/05
5. Kurapov, Yu.A., Romanenko, S.M., Didikin, G.G., Oranskaya, E.I. (2017) Controllable synthesis of iron oxide nanoparti cles in porous NaCl matrix. Materials Research Express, 4(3), 035031. https://doi.org/10.1088/2053-1591/4/3/035031
6. Paton, B.E., Movchan, B.O., Kurapov, Yu.A., Yakovchuk, K.Yu. (2010) Method of producing of metal-oxygen system nanoparticles with specified composition by electron beam evaporation and condensation in vacuum. Pat. 92556, Ukraine [in Ukrainian]. http://base.ukrpatent.org/searchINV/search. php?action=viewdetails&IdClaim=151646
7. Grechanyuk, M.I., Osokin, V.O., Afanasiev, I.B. et al. (2002) Method of producing of porous materials. Pat. 46855, Ukraine [in Ukrainian].
8. Grechanyuk, N.I., Osokin, V.A., Grechanyuk, I. N. et al. (2006) Composite materials on base of copper and molybdenum condensed from vapor phase, for electric contacts. Pt 2: Fundamentals of electron beam technology for producing materials for electric contacts. Advances in Electrometallurgy, 2, 8-17.
9. Osokin, V.O., Kurapov, Yu.A., Boretsky, V.V. et al. (2021) Producing of Fe, Cu, Ag nanoparticles in NaCl matrix on rotating substrate by EB-PVD method. In: Abstr. of Pap. of Int. Conf. on Modern Technologies of Joining of Materials. Ed. by L.M. Lobanov. Kyiv, IAW [in Russian]. https://patonpublishinghouse. com/proceedings/stzm2021.pdf
10. Movchan, B.A. (2006) Inorganic materials and coating produced by EBPVD. Surf. Eng., 22, 35-46. https://doi.org/10.1179/174329406X85029
11. Movchan, B.A., Demchishin, A.V. (1969) Study of structure and properties of thick vacuum condensates of nickel, titanium, tungsten, aluminium oxide and zirconium dioxide. Fizika Metallov i Metallovedenie, 28(4), 653-660 [in Russian].
12. Kurapov, Y.A., Vazhnichaya, E.M., Litvin, S.E. et al. (2019) Physical synthesis of iron oxide nanoparticles and their biological activity in vivo. SN Applied Sci., 1(1), 1-102. https://doi.org/10.1007/s42452-018-0110-z
13. Kurapov, Yu.A., Movchan, B.A., Litvin, S.E. et al. (2011) Effect of iron concentration on the adsorptive capacity of iron oxide nanoparticles in the porous NaCl matrix in relation to atmospheric oxygen. Advances in Electrometallurgy, 9(1), 29-32. http://pwi-scientists.com/pdf/journals/aiem201101.pdf

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